VALIDASI METODE ANALISIS POLISIKLIK AROMATIK HIDROKARBON (PAH) DALAM SEDIMEN DI SEKITAR PANTAI MAKASSAR
Abstract: Validation of analysisÂ
method of PAH have been done in marine sediment of Macassar Coast by Gas
Chromatography (GC-FID). Validation of method include:Â limit of detection (LoD), limit of
quantification (LoQ) and linearity range. The results of validation method of 7
types PAHs (Naphtalene, Acenaphtene, Penanthrene, Fluoranthene, Pyrene, Benzo
(a) Anthracene and perylene) giveÂ
a linearity range between 0.5 to 20 ppm with an average
linearity approaches a value of 1. LoD forÂ
Naphtalene; Acenaphthene; Penanthrene; Fluoranthene; Pyrene; Benzo (a)
Anthracene; and Perylene are 3.541;
0.208; 1,736; 1.737; 1,738; 12.124; and 2,128 ppm, respectively. LoQ for
Naphtalene; Acenaphthene; Penanthrene; Fluoranthene; Pyrene; Benzo (a)
Anthracene; and Perylene are 11,803;
0.695; 5.786; 5.786; 5.788; 5.794; 7.0796 and 7.092 ppm, respectively. Limit of
detection (LoD), limit of quantification (LoQ), linearity and linear range can
be used to determine the concentration of PAH in sediment samples.
Penulis: Muhammad Syahrir, Nurul
Hidayat Aprilita, nuryono
Kode Jurnal: jpkimiadd150636
